Ep. 13: Maka and Soul struggle with diverging wavelengths while fighting Free the immortal werewolf in London.

Stein subjects Maka and Soul to emotional stimulant training that exposes their flaws, causing an argument that threatens their resonance. They later attend a supplementary class in London with Black Star and Tsubaki, where they encounter Free, an immortal werewolf released from Witch Prison by Eruka for Medusa. During a battle on a suspension bridge, Black Star collapses after using Tsubaki's Enchanted Sword mode, leaving Maka and Soul to fight alone. Their diverging soul wavelengths cause Soul to burn Maka's hands in weapon form, rendering him difficult to control. Tsubaki persuades them to reconcile, restoring their resonance but intensifying the madness of Soul's black blood. Maka defeats Free with her Witch Hunter, aided by the revived Black Star. Afterward, Maka coughs black blood into her hand.
Episodes
- Ep. 9 · Black Star and Kid search for the arrogant Holy Sword Excalibur while Death Scythe explains the Demon Sword's danger to Maka.
- Ep. 10 · Black Star and Tsubaki confront Masamune, the soul-devouring Enchanted Sword, in a hostile village.
- Ep. 11 · Tsubaki battles Masamune within the Enchanted Sword and absorbs her first soul
- Ep. 12 · Maka Albarn resolves her fear of Soul's injury while Medusa deals with rebellious witches.
- Ep. 13 · Maka and Soul struggle with diverging wavelengths while fighting Free the immortal werewolf in London.
- Ep. 14 · The Super Written Exam: Heart-pounding, Reeling, and Restless. You're Kidding!?
- Ep. 15 · Kid investigates the Black Dragon on the Nidhogg ship while Liz meets spirits and Crona arrives.
- Ep. 16 · Kid fights Crona on a ghost ship while Maka and Stein investigate Medusa's black blood scheme
- Ep. 17 · Ox encounters the eccentric Excalibur and hears his thousand rules before rejecting him.